|
Module Number:
| 13314
|
| Module Title: | Instrumental Analysis and Physical Chemistry |
| |
Instrumentelle Analytik und physikalische Chemie
|
| Department: |
Faculty 2 - Environment and Natural Sciences
|
| Responsible Staff Member: | -
apl. Prof. Dr. rer. nat. Schmid, Reiner
|
| Language of Teaching / Examination: | English |
| Duration: | 1 semester |
| Frequency of Offer: |
Every summer semester
|
| Credits: |
6
|
| Learning Outcome: | Part 1: Introduction to modern instrumental analytical techniques
The student gets an overview of the most important instrumental analytical methods and their fields of application.
After completing the module, the student is able
- to understand the physical relationships that provide the theoretical foundations of instrumental analysis.
- to evaluate instrumental analytical methods with respect to their performance and their scope of application.
- to interpret/evaluate spectroscopic and chromatographic data.
- to derive structures of simple organic compounds from spectroscopic data.
Part 2: Introduction to Physical Chemistry
The student gets an overview of the most important concepts of classical physical chemistry.
The student achieves:
- the ability, to connect different subdisciplines of physical chemistry, due to their understanding of important common concepts.
- an overview which could be adapted to other fields.
- the ability, to solve simple problems out of the respective topics.
- interdisciplinary knowledge, due to inclusion of practical examples from different technological areas.
|
| Contents: | Part 1:
Introduction to Instrumental Analysis
- Performance characteristics of different methods
- Errors in Analytical Chemistry
Separation Techniques
- Fundamentals of Chromatography
- Gas Chromatography (GC)
- High Performance Liquid Chromatography (HPLC)
- Thin-Layer Chromatography (DC)
- Size-Exclusion Chromatography (SEC)
Mass-Spectrometry
- General
- Ionisation Methods
- Mass-Analyzers and Detectors
- Interpretation of Mass-Spectra
Spectroscopic Methods
- Characteristics of Electromagnetic Radiation
- Introduction to Spectroscopy
- Infrared (MIR) – Absorption-Spectroscopy
- Ultraviolet/visible (UV/VIS) – Absorption-Spectroscopy
- Fluorescence; Phosphorescence and Chemoluminescence
- Atomic Absorption (AAS) / Atomic Emission (AES)
Part 2:
Thermodynamics
- The properties of gases, ideal gas equation, van der Waals equation
- 1st law of thermodynamics, internal energy, work and heat, enthalpy, heat capacity, Carnot cycle, Joule Thomson effect, liquefaction of gases
- thermochemistry, Hess’s law, temperature dependence of reaction enthalpy (Kirchhoff’s law), calorimetry
- 2nd law, entropy, heat engines, Gibbs energy, chemical potential
Physical transformations of pure substances
- Phase diagrams, phase boundaries, Clausius-Clapeyron equation
Properties of simple mixtures
- Chemical potential of liquids, Raoult’s law, Henry’s law, Colligative properties, Phase diagram of mixtures
Chemical equilibrium
- Gibbs energy minimum, relation of Gibbs energy and the equilibrium constant
Chemical kinetics
- Rates of reactions, integrated rate laws, first-order reactions, half-lives, radiocarbon dating, temperature dependence of reaction rates (Arrhenius equation), relation of equilibrium constant and the rates of reaction
|
| Recommended Prerequisites: | Knowledge about: Basics in Physics and Chemistry |
| Mandatory Prerequisites: | None |
| Forms of Teaching and Proportion: | -
Lecture
/ 4 Hours per Week per Semester
-
Exercise
/ 2 Hours per Week per Semester
-
Tutorial
/ 1 Hours per Week per Semester
-
Self organised studies
/ 75 Hours
|
| Teaching Materials and Literature: | Part 1:
- P. W. Atkins: Physical Chemistry (Oxford University Press),
- Laidler/Meiser/Sanctuary: Physical Chemistry (Houghton, Mifflin),
Part 2:
- R. Kellner: Analytical Chemistry (Wiley-VCH),
- Skoog, Leary: Instrumentelle Analytik (Springer Verlag)
|
| Module Examination: | Final Module Examination (MAP) |
| Assessment Mode for Module Examination: | Written exam at the end of the semester (120 min; graded)
|
| Evaluation of Module Examination: | Performance Verification – graded |
| Limited Number of Participants: | None |
| Part of the Study Programme: | -
Master (research-oriented) /
Angewandte Mathematik /
PO 2008
-
Master (research-oriented) /
Angewandte Mathematik /
PO 2019
-
Bachelor (research-oriented) /
Architektur /
PO 2014
-
Bachelor (research-oriented) - Double Degree /
Architektur /
PO 2014
-
Bachelor (research-oriented) /
Architektur /
PO 2022
-
Master (research-oriented) /
Architektur /
PO 2016
-
Master (research-oriented) /
Artificial Intelligence /
PO 2022
-
Master (research-oriented) /
Bauen und Erhalten /
PO 2007
-
Abschluss im Ausland /
Bauingenieurwesen /
keine PO
-
Bachelor (research-oriented) - Extended Semester /
Bauingenieurwesen /
PO 2017
-
Bachelor (research-oriented) /
Bauingenieurwesen /
PO 2017
-
Bachelor (research-oriented) /
Bauingenieurwesen /
PO 2022
-
Bachelor (research-oriented) - Extended Semester /
Bauingenieurwesen /
PO 2022
-
Master (research-oriented) /
Bauingenieurwesen /
PO 2014
-
Bachelor (research-oriented) - Co-Op Programme with Integrated Vocational Training /
Bauingenieurwesen - dual /
PO 2017
-
Bachelor (research-oriented) - Co-Op Programme with Integrated Vocational Training /
Bauingenieurwesen - dual /
PO 2022
-
Bachelor (research-oriented) - Co-Op Programme with Practical Placement /
Bauingenieurwesen - dual /
PO 2022
-
Bachelor (research-oriented) /
Bau- und Kunstgeschichte /
PO 2022
-
Bachelor (applied) /
Betriebswirtschaftslehre /
PO 2017
-
Bachelor (research-oriented) /
Betriebswirtschaftslehre /
PO 2011
-
Bachelor (research-oriented) /
Betriebswirtschaftslehre /
PO 2017
-
Bachelor (research-oriented) /
Betriebswirtschaftslehre /
PO 2024
-
Master (research-oriented) /
Betriebswirtschaftslehre /
PO 2017
-
Bachelor (applied) - Co-Op Programme with Practical Placement /
Betriebswirtschaftslehre - dual /
PO 2019
-
Bachelor (research-oriented) - Co-Op Programme with Practical Placement /
Betriebswirtschaftslehre - dual /
PO 2024
-
Abschluss im Ausland /
Biotechnologie /
keine PO
-
Bachelor (applied) /
Biotechnologie /
PO 2018
-
Bachelor (applied) - Double Degree /
Biotechnologie /
PO 2021
-
Master (applied) /
Biotechnology /
PO 2018
-
Master (applied) - Extended Semester /
Biotechnology /
PO 2018
-
Master (research-oriented) /
Cyber Security /
PO 2017
-
Bachelor (research-oriented) /
Digitale Gesellschaft /
PO 2022
-
Bachelor (research-oriented) /
eBusiness /
PO 2007
-
Master (research-oriented) /
eBusiness /
PO 2007
-
Bachelor (applied) /
Elektrotechnik /
PO 2018
-
Bachelor (research-oriented) /
Elektrotechnik /
PO 2014
-
Bachelor (research-oriented) /
Elektrotechnik /
PO 2019
-
Bachelor (research-oriented) /
Elektrotechnik /
PO 2022
-
Master (applied) /
Elektrotechnik /
PO 2018
-
Master (applied) - Extended Semester /
Elektrotechnik /
PO 2018
-
Master (research-oriented) /
Elektrotechnik /
PO 2014
-
Master (research-oriented) /
Elektrotechnik /
PO 2019
-
Master (research-oriented) /
Elektrotechnik /
PO 2023
-
Bachelor (applied) - Co-Op Programme with Integrated Vocational Training /
Elektrotechnik - dual /
PO 2018
-
Bachelor (applied) - Co-Op Programme with Practical Placement /
Elektrotechnik - dual /
PO 2018
-
Bachelor (research-oriented) - Co-Op Programme with Integrated Vocational Training /
Elektrotechnik - dual /
PO 2022
-
Bachelor (research-oriented) - Co-Op Programme with Practical Placement /
Elektrotechnik - dual /
PO 2022
-
Abschluss im Ausland /
Environmental and Resource Management /
keine PO
-
Bachelor (research-oriented) /
Environmental and Resource Management /
PO 2015
-
Bachelor (applied) /
Hebammenwissenschaft /
PO 2021
-
Bachelor (applied) - Co-Op Programme with Integrated Vocational Training /
Hebammenwissenschaft /
PO 2021
-
Bachelor (research-oriented) /
Informatik /
PO 2008
-
Master (research-oriented) /
Informatik /
PO 2008
-
Bachelor (research-oriented) /
Informations- und Medientechnik /
PO 2017
-
Master (research-oriented) /
Informations- und Medientechnik /
PO 2017
-
Bachelor (applied) /
Instrumental- und Gesangspädagogik /
PO 2019
-
Bachelor (research-oriented) /
Kultur und Technik /
PO 2017
-
Master (research-oriented) /
Kultur und Technik /
PO 2017
-
Bachelor (research-oriented) /
Künstliche Intelligenz /
PO 2022
-
Bachelor (research-oriented) /
Künstliche Intelligenz Technologie /
PO 2022
-
Master (research-oriented) /
Künstliche Intelligenz Technologie /
PO 2022
-
Bachelor (research-oriented) /
Landnutzung und Wasserbewirtschaftung /
PO 2017
-
Master (research-oriented) /
Landnutzung und Wasserbewirtschaftung /
PO 2011
-
Master (research-oriented) /
Landnutzung und Wasserbewirtschaftung /
PO 2018
-
Bachelor of Education /
Lehramt Primarstufe /
PO 2023
-
Master (research-oriented) /
Leichtbau und Werkstofftechnologie /
PO 2023
-
Master (research-oriented) - Co-Op Programme with Practical Place /
Leichtbau und Werkstofftechnologie - dual /
PO 2023
-
Bachelor (applied) /
Maschinenbau /
PO 2018
-
Bachelor (research-oriented) /
Maschinenbau /
PO 2006
-
Bachelor (research-oriented) /
Maschinenbau /
PO 2021
-
Master (applied) /
Maschinenbau /
PO 2018
-
Master (applied) - Extended Semester /
Maschinenbau /
PO 2018
-
Master (research-oriented) /
Maschinenbau /
PO 2006
-
Master (research-oriented) /
Maschinenbau /
PO 2023
-
Master (research-oriented) - Reduced Semester /
Maschinenbau /
PO 2023
-
Bachelor (applied) - Co-Op Programme with Integrated Vocational Training /
Maschinenbau - dual /
PO 2018
-
Bachelor (applied) - Co-Op Programme with Practical Placement /
Maschinenbau - dual /
PO 2018
-
Bachelor (research-oriented) - Co-Op Programme with Integrated Vocational Training /
Maschinenbau - dual /
PO 2021
-
Bachelor (research-oriented) - Co-Op Programme with Practical Placement /
Maschinenbau - dual /
PO 2021
-
Master (research-oriented) - Co-Op Programme with Practical Place /
Maschinenbau - dual /
PO 2023
-
Bachelor (research-oriented) /
Materialchemie /
PO 2018
-
Master (research-oriented) /
Materialchemie /
PO 2018
-
Bachelor (research-oriented) /
Mathematik /
PO 2019
-
Bachelor (research-oriented) /
Mathematik /
PO 2023
-
Bachelor (research-oriented) - Co-Op Programme with Practical Placement /
Mathematik - dual /
PO 2023
-
Bachelor (research-oriented) /
Medizininformatik /
PO 2016
-
Bachelor (research-oriented) /
Medizintechnik /
PO 2022
-
Bachelor (research-oriented) - Co-Op Programme with Practical Placement /
Medizintechnik - dual /
PO 2022
-
Master (research-oriented) /
Nachwachsende Rohstoffe und Erneuerbare Energien /
PO 2008
-
No Final Exam Possible /
Orientierungsstudium (1 Semester) /
PO 2022
-
No Final Exam Possible /
Orientierungsstudium (2 Semester) /
PO 2022
-
Bachelor (applied) /
Pflegewissenschaft /
PO 2017
-
Bachelor (applied) /
Pflegewissenschaft /
PO 2020
-
Bachelor (applied) - Co-Op Programme with Integrated Vocational Training /
Pflegewissenschaft /
PO 2020
-
Master (research-oriented) /
Physics /
PO 2021
-
Abschluss im Ausland /
Physik /
keine PO
-
Bachelor (research-oriented) /
Physik /
PO 2021
-
Master (research-oriented) /
Physik /
PO 2018
-
Master (research-oriented) /
Power Engineering /
PO 2016
-
Bachelor (applied) /
Soziale Arbeit /
PO 2018
-
Bachelor (applied) - Double Degree /
Soziale Arbeit /
PO 2018
-
Bachelor (applied) /
Soziale Arbeit /
PO 2020
-
Bachelor (applied) - Double Degree /
Soziale Arbeit /
PO 2020
-
Master (applied) /
Soziale Arbeit /
PO 2018
-
Master (applied) /
Soziale Arbeit /
PO 2020
-
Bachelor (applied) /
Therapiewissenschaften /
PO 2017
-
Bachelor (research-oriented) /
Umweltingenieurwesen /
PO 2006
-
Bachelor (research-oriented) /
Umweltingenieurwesen /
PO 2021
-
Master (research-oriented) - Double Degree /
Verarbeitungstechnologien der Werkstoffe /
PO 2015
-
Bachelor (research-oriented) /
Verfahrenstechnik /
PO 2013
-
Bachelor (applied) /
Wirtschaftsingenieurwesen /
PO 2018
-
Master (applied) /
Wirtschaftsingenieurwesen /
PO 2018
-
Master (applied) - Extended Semester /
Wirtschaftsingenieurwesen /
PO 2018
-
Bachelor (applied) - Co-Op Programme with Integrated Vocational Training /
Wirtschaftsingenieurwesen - dual /
PO 2018
-
Bachelor (applied) - Co-Op Programme with Practical Placement /
Wirtschaftsingenieurwesen - dual /
PO 2018
-
Bachelor (research-oriented) /
Wirtschaftsmathematik /
PO 2007
-
Bachelor (research-oriented) /
Wirtschaftsmathematik /
PO 2023
-
Bachelor (research-oriented) - Co-Op Programme with Practical Placement /
Wirtschaftsmathematik - dual /
PO 2023
|
| | This module has been approved for the general studies. |
| Remarks: | None |
| Module Components: | - 228450 Lecture Instrumental Analysis and Physical Chemistry
- 228451 Exercise Instrumental Analysis and Physical Chemistry
- 228454 Tutorial Instrumental Analysis and Physical Chemistry
- 228455 Exam Instrumental Analysis and Physical Chemistry
- 228456 Exam/Repetition Instrumental Analysis and Physical Chemistry
|
| Components to be offered in the Current Semester: | |
