14327 - Crystal Chemistry and Crystal Growth Modulübersicht

Module Number: 14327
Module Title:Crystal Chemistry and Crystal Growth
  Kristallchemie und Kristallzüchtung
Department: Faculty 2 - Environment and Natural Sciences
Responsible Staff Member:
  • Prof. Dr. rer. nat. habil. Schmidt, Peer
Language of Teaching / Examination:English
Duration:1 semester
Frequency of Offer: Every summer semester
Credits: 6
Learning Outcome:After completing the module, the students will be able to recognize the connection between phase diagrams and crystallization pathways. They are also able to describe the crystalline state and the typical crystal structures of inorganic solids and materials. With the help of the acquired knowledge of the thermodynamics and kinetics of crystal growth processes, students gain a rational approach to methods of crystallization of inorganic solids and materials.
 
Students reflect on the lecture material and are able to discuss relevant scientific problems in crystal chemistry. With reference to current issues, they can carry out literature research and open up scientific publications and reports. They are able to combine different concepts relating to crystal growth processes and the formation of ideal and real structures of solids. Students can work together in small working groups, develop solutions to given problems and present their results orally and in writing.
 
Students are also able to transfer their knowledge to simple modeling approaches and laboratory work. They are able to familiarize themselves independently with an experimental topic, plan work processes under given conditions, organize themselves in a laboratory group and carry out chemical experiments. Finally, they can save experimental data, document their work in reports and communicate in presentations.
 
The specialist knowledge in theory and laboratory work provides students with in-depth knowledge of crystal growth processes and crystal structures of inorganic solids and materials and qualifies them for further collaboration in scientific research as well as in application-oriented research and development of new materials.
Contents:Lecture:
- The crystalline state and crystal structures of inorganic solids
- Existence ranges of inorganic solids and pathways to their crystallization
- Thermodynamic fundamentals of phase diagrams of inorganic solids and basics for their thermochemical modelling
- Nucleation and crystal growth
- Methods of crystal growth in the laboratory and in industrial practice
- Applications of crystalline solids as functional materials
 
Exercise:
- Calculation of phase diagrams with simple spreadsheets
- Calculation/modelling of phase diagrams by Calphad-method
- Calculation/modelling of crystallization pathways
 
Practical course
- Methods of crystal growth in the laboratory and in industrial practice
- Chemical analysis of crystalline materials
- Fundamentals of crystal structure analysis
Recommended Prerequisites:Knowledge of the topics/basic courses in general chemistry, inorganic chemistry, physical chemistry,
instrumental analytics
Mandatory Prerequisites:None
Forms of Teaching and Proportion:
  • Lecture / 2 Hours per Week per Semester
  • Exercise / 1 Hours per Week per Semester
  • Practical training / 2 Hours per Week per Semester
  • Self organised studies / 105 Hours
Teaching Materials and Literature:
  • U. Müller, Inorganic Structural Chemistry (Inorganic Chemistry, Band 22), Wiley & Sons Inc; 2. Edition (2006), ISBN: ‎ 978-0470018644.
  • G. Dhanaraj (Edt.), Springer Handbook of Crystal Growth, Springer; 2010, ISBN-13 ‏ : ‎ 978-3540741824
  • M. Binnewies, R. Glaum, M. Schmidt, P. Schmidt, Chemical Vapor Transport reactions, Verlag: De Gruyter; 1. Auflage 2012; ISBN: 978-3110254648.
  • A.R. West, Solid State Chemistry and its Applications, Wiley & Sons; 2. Edition, 2022, ISBN: ‎ 978-1118447444
Module Examination:Prerequisite + Final Module Examination (MAP)
Assessment Mode for Module Examination:Prerequisite:
  • Successful completion of the practical course
  • Successful completion of exercises
Final module examination:
  • Written examination, 120 min.
Evaluation of Module Examination:Performance Verification – graded
Limited Number of Participants:None
Part of the Study Programme:
  • no assignment
Remarks:No offer in 2025.
Module Components:
  • Lecture crystal chemistry
  • Exercise crystal chemistry
  • Practical course in solid state chemistry
  • Module examination (written exam)
Components to be offered in the Current Semester:
  • no assignment